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1.000 g of soil, as-received, gave a moisture content of 14.00%. The oven-dried sample, completely moisture-free, showed 18.00% K. Find the percentage of K in the sample as received.
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- 13. A fish meal sample has the following composition: protein 20%, moisture 12%, additive 66%. The sample is placed in a drying oven and subsequent analysis gave a value of 22% protein. Calculate the % moisture content of the dried sample. 14. 1.000 g of soil, as-received, gave a moisture content of 14.00%. The oven-dried sample, completely moisture-free, showed 18.00% K. Find the percentage of K in the sample as received.Which statement about the determination of the percentage purity of benzoic acid is correct? * A- Only sodium hydroxide solution can be used as the titrant in the volumetric analysis of benzoic acid. B- Analysing a benzoic acid sample that still contains some hydrochloric acid may yield an analyte percentage that is less than expected. C- Analysing a wet benzoic acid sample may yield an analyte percentage that is more than expected. D- All these statements are correct. E- None of these statements are correct.You are given a 1:1 (by weight) solid mixture of vitamin C and vitamin A, and you are going to use liquid-liquid extraction to separate one from the other (chemical structures are given below). If you decide to use water (density, 1 g/mL) and ethanol (density, 0.789 g/mL) as your extraction solvents, will this separation be successful? Why or why not? он HO HO. HO HO Vitamin C (ascorbic acid) Vitamin A (retinol)
- You obtain an Unknown Sample from the Stockroom. You begin testing the solution through the steps outlined in the flowchart of the experiment’s PDF file. You first add HCl and centrifuge your mixture. You observe the formation of a white precipitate in the bottom of the test tube. After pouring off the supernatant liquid, you add hot water to the white precipitate. Addition of the hot water dissolves some of the precipitate, but some white precipitate still remains on the bottom of the test tube. You pour off the supernatant liquid, and add ammonia (NH3) to the remaining precipitate. You now observe the formation of a gray-black precipitate. Which of the following is a valid conclusion to draw at this point? Select one: Hg22+ is definitely present. Pb2+ is definitely present. Ag+ could be present, or Hg22+ could be present, or BOTH could be present. Ag+ is definitely presentYou obtain an Unknown Sample from the Stockroom. You begin testing the solution through the steps outlined in the flowchart of the experiment’s PDF file. You first add HCl and centrifuge your mixture. You observe the formation of a white precipitate in the bottom of the test tube. After pouring off the supernatant liquid, you add hot water to the white precipitate. Addition of the hot water dissolves some of the precipitate, but some white precipitate still remains on the bottom of the test tube. Which of the following is a valid conclusion to draw at this point? Pb2+ is definitely present. Hg22+ is definitely present. Ag+ could be present, or Hg22+ could be present, or BOTH could be present. Ag+ is definitely presentYou obtain an Unknown Sample from the Stockroom. You begin testing the solution through the steps outlined in the flowchart of the experiment’s PDF file. You first add HCl and centrifuge your mixture. You observe the formation of a white precipitate in the bottom of the test tube. After pouring off the supernatant liquid, you add hot water to the white precipitate. Upon addition of the hot water, you have some white precipitate still at the bottom of the test tube, and the supernatant liquid is poured off. To this liquid, potassium chromate (K2CrO4) is added. Upon this addition of potassium chromate, you observe no formation of precipitate. Which of the following is a valid conclusion to draw at this point? (Choose one.) Select one: 1. Hg22+ is definitely present. 2. Pb2+ is NOT present. 3. Ag+ is definitely present. 4. Pb2+ is definitely present.
- The thiourea in a 1.455 g sample of organic material was extracted into a dilute sulfuric acid solution and titrated with 37.31 mL of 0.009372 M Hg2+ via reaction: 4(NH2)2CS + Hg2+ →[(NH2)2CS]4 Hg2+ Is this an example of total analysis technique or concentration technique? Explain. Calculate the percent (NH2)2CS ( 76.12 g/mol) in the sample. What is classification of the analysis based on the amount of sample and amount of analytes present? Explain.Color BEFORE adding Color AFTER adding Intensity of color AFTER adding FeCl3 Test Tube # FeCl3 FeCl3 #1 (salicylic acid) clear lilac 100% #2 (commercial aspirin A) clear slightly pink 50% #3 (commercial aspirin B) clear lilac 95% #4 (aspirin from your clear pink 20% synthesis above) #5 (control) clear clear 0% Based on this data and the melting point of Aspirin, how pure is the synthesized product?A 5.000-g soil sample was analyzed for potassium content by extracting the potassium using 10.00 mL aqueous ammonium acetate solution. Following the extraction, the soil was filtered and rinsed. The filtrate with rinsings was diluted to exactly 50.00 mL. Then, 1.00 mL of this solution was diluted to 25.00 mL, and this dilution was tested with an instrument. The concentration in this 25.00 mL was found to be3.18 ppm. What is the concentration of the potassium in the soil in ppm?
- 25 ml of pickled brine was taken from an apple pickled with vinegar and diluted to 500 ml, 25 ml of this was taken and acidity was determined with 0.2 N (Factor: 1.05) NaOH. In the main trials, 6.3 ml - 6.5 ml - 6.9 ml, respectively, 0.1 ml base was used in the analysis without using the sample.For example, how many ppm is its acidity?To quantify the amount of ethanol in a beverage, a technician prepared the first solution which contained 4.90 grams unknown, 1.00 grams acetonitrile, and 4.10 grams water. After the GC analysis which reported the peak areas of 5,742 for ethanol and 3,829 for acetonitrile, the technician added 0.20 grams ethanol to the first solution and ran the GC analysis again. This time, the peak areas of 6,382 for ethanol and 3,709 for acetonitrile for solution 2 were obtained. What was the percent by mass ethanol in the original beverage?D. Solvent Extraction Samples Upper phase Lower phase Oil + Water Kerosene + Oil