Complete the spectroscopy data tables for a compound with molecular formula C6H14. Determine the structure of the compound. Any labile protons, if they exist, will not be present in this particular 1H NMR spectrum.
Complete the spectroscopy data tables for a compound with molecular formula C6H14. Determine the structure of the compound. Any labile protons, if they exist, will not be present in this particular 1H NMR spectrum.
Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter19: Nuclear Magnetic Resonance Spectroscopy
Section: Chapter Questions
Problem 19.32QAP: The proton NMR spectrum in Figure 19-40 is for a compound having an empirical formula C4H7BrO2....
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Question
Complete the spectroscopy data tables for a compound with molecular formula C6H14.
Determine the structure of the compound. Any labile protons, if they exist, will not be
present in this particular 1H NMR spectrum.
![4 Degrees of Unsaturation (show work):
DOU =0
[2 (6) + 2 -14+0 -0]
2
IR Data Table
13C NMR Data Table
Stretch (cm)
BC Signal Chemical Shift (ppm) 1°C Signal Chemical Shift (ppm)
Bond
C-H sp
1
34 ppana
~ 3000 cm
2.
18
'H NMR Data Table
H Signal
Chemical Shift (ppm)| Integration
Multiplicity
A
1.41 pem
Proposed Structure
6H
H,C-C-C-CH3
CHz CHz](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2F41ea191e-828c-4f9d-b6fb-1ac8fc340597%2F3a44a41c-aa42-415e-a294-5569d3817b30%2F2thmiuc_processed.jpeg&w=3840&q=75)
Transcribed Image Text:4 Degrees of Unsaturation (show work):
DOU =0
[2 (6) + 2 -14+0 -0]
2
IR Data Table
13C NMR Data Table
Stretch (cm)
BC Signal Chemical Shift (ppm) 1°C Signal Chemical Shift (ppm)
Bond
C-H sp
1
34 ppana
~ 3000 cm
2.
18
'H NMR Data Table
H Signal
Chemical Shift (ppm)| Integration
Multiplicity
A
1.41 pem
Proposed Structure
6H
H,C-C-C-CH3
CHz CHz
Transcribed Image Text:7) Complete the spectroscopy data tables for a compound with molecular formula C6H14.
Determine the structure of the compound. Any labile protons, if they exist, will not be
present in this particular 'H NMR spectrum.
50
4000
3000
2000
15D0
1000
500
HAVENUMB ER l-
1.38
1.36 1.34
1.32
1.42
1.40
f1 (ppm)
1.48
1.46
1.44
1.7
1.6 1.5
1.3
1.2
1.1
1.0
0.9
0.8
0.7
0.6
f1 (ppm)
130 120 110 100
f1 (ppm)
90
80
70
60 50
40
30
20
10
TRANSMITTANCEII
*1.01-
-66'의
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