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- Standardization of EDTA solution
|
Trial number |
Volume of EDTA used (mL) |
|
1 |
9.7 |
|
2 |
8.9 |
|
3 |
9.4 |
Calculate Average Molarity of EDTA and Relative Average Deviation (R.A.D.)
- Hardness Titration
|
Trial number |
Volume of EDTA used (mL) |
|
1 |
12.2 |
|
2 |
12.6 |
|
3 |
11.6 |
Average ppm CaCO3 and Relative Average Deviation (R.A.D.) I need.
M(Ca2+)+V(Ca2+)->M(EDTA)+V(EDTA)
0,01M + 10ml -> ? + V(EDTA)
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- . 100 ml boiled cooled and filtered water sample takes 9.6 ml of M/50 EDTA in titration. The Permanent hardness of the water sample in terms of ppm of CaCO3 equivalent is10) 1.0 gram of CaCO3 was dissolved in HCl and the solution was made up to 1000 ml with distilled water. 50 ml of the solution required 45 ml of EDTA solution for titration, 50 ml of hard water sample required 28 ml of EDTA and after boiling and filtering required 15 ml of EDTA solution. Calculate Temporary Hardness. A. 288.6 ppmB. 166.6 ppmC. 88.6ppm 11) Calculate the Permanent Hardness for No. 10 A. 111 ppmB. 222 ppmC. 333 ppm 12) Calculate the Total Hardness for No. 10 A. 421.6 ppmB. 621.6 ppmC. 521.6 ppmFelodipine calcium channel blocker standard (0.251mg/ml) and felodipine sample (0.245mg/ml) solutions were prepared and injected to the HPLC. The peak area of felodipine standard is 275428 and the sample is 272982. The potency (purity) of felodipine standard is 98.9%. What is the assay percentage of felodipine? a. 102.23 b. 98.71 c. 101.07 d. 100.42
- Calculate the water hardness (mg L-1 of CaCO3) (i.e. calculate the mass of CaCO3) please show working out. thank you :) Sample No. 1 2 3 4 Final Burette reading (mL) 24.40 46.90 24.70 47.20 Initial Burette reading (mL) 0.10 24.40 2.10 24.70 Final-Initial Titre (mL) 24.30 22.50 22.60 22.50A fish sample was analyzed for crude protein content using the Kjeldahl method. Thefollowing data were recorded: Moisture content 10.0%Weight of sample 2.15 gNormality of HCl used for titration 0.121 NHCl used for sample 28.5 mLHCl used for reagent blank 0.2 mL Calculate crude protein content on wet weight basis of the fish sample, assuming fishprotein contains 20% nitrogen.Conc. of NaOH: TRIAL 1 TRIAL 2 TRIAL 3 Mass of flask 81.061 g 69.692 g 96.039 g Mass of flask and vinegar 83.010 g 71.578 g 97.940 g Mass of vinegar 1.949 g 1.886 g 1.901 g Volume of vinegar 2.00 mL 2.00 mL 2.00 mL Initial buret reading Final buret reading 17.0 mL 17.5 mL 16.0 mL Volume of NaOH delivered 17.0 mL 17.5 mL 16.0 mL Moles of NaOH delivered 0.0325 moles 0.0314 moles 0.0317 moles Moles of acetic acid in vinegar 0.0016 moles 0.0016 moles 0.0016 moles Mass of acetic acid in vinegar 0.097 g 0.094 g 0.095 g Molarity of acetic acid in vinegar 0.811 M 0.785 M 0.791 M Average molarity of acetic acid 0.796 M % by mass of acetic acid in vinegar Average % mass of acetic acid in vinegar Standard deviation of % mass acetic acid
- Concentration EDTA (M): 1.94e-3 Trial #1 Trial #2 Trial #3 Volume of Water Sample titrated (mL): 25.00 25.00 25.00 Volume EDTA used (mL): 36.23 39.00 37.77 Calculate the average of the volume of EDTA used. Calculate the number of moles of EDTA solution required to titrate the water sample. The total hardness is due to one or a combination of Ca2+, Mg2+, and Fe2+ in your sample. It is convenient to express this hardness as though it was entirely due to Ca2+. Making this assumption, determine the number of moles of Ca2+ present in the bottled water sample. The total hardness and the information on Table 1 is always listed in parts-per-million (ppm) of CaCO3 (or mg CaCO3/KgH2O). Since the density of water is 1.0 g/mL, one ppm would be the same as the number of mg of CaCO3 per liter of water. Determine the number of moles of CaCO3 present in the bottled water, assuming all the Ca2+ combine with CO32−. Calculate the number of grams of CaCO3 present and convert to mg.…Ooldtion Table 1. Measurements for standardization of NaOH Trial 1 Trial 2 Trial 3 1] Tared mass of KHC3H4O4 (9) 0.374 0.325 0.357 12] Burette reading of NaOH, initial (mL) 4.59 3.61 4.03 [3] Burette reading of NaOH, final (mL) 22.03 18.77 21.17 Part B. Molar Concentration of an Acid Solution Enter the number corresponding to the type of acid you have 1. HA 3 2. H2A 3. H3A Enter the unknown number. 21 Table 2. Measurements for titration of unknown acid Trial 1 Trial 2 Trial 3 [1] Volume of acid (mL) 25.0 25.0 25.0 [2] Burette reading of NaOH, initial (mL) 2.13 2.48 3.68 [3] Burette reading of NaOH, final (mL) 24.10 24.52 25.56 Part C. Percentage by Mass of an Unknown Solid Enter the number corresponding to the type of acid you have 1. HA 3 2. H2A 3. H3A Enter the unknown number. 30 Molar mass of the unknown acid 192.14 Table 3. Measurements for titriation of solid Trial 1 Trial 2 Trial 3 [1] Mass of sample (g) 26.334 29.157 27.111 [2] Burette reading of NaOH, initial (mL) 3.21 1.48…Volume of dye solution added (mL) 9.80 mL Concentration of bleach solution used (M) 0.090 M Volume of bleach solution added (mL) 0,20 mL. Total Volume of solution (mL) 10.0 mL O5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 ABS Ln Abs = -4.860e-2 t + 1.35e-1 0.0 INABS -0.2 -0.4 1/ABS -0.6 -0.8 -1.0 -1.2 -1.4 Time (s) -1.6 b) From the data above, what are the initial molar concentrations of [dye] and [bleach] for your experiment? (NOTE: The concentration of the stock yellow dye solution is 3.40x10 M) [dye)o (M) [bleach]o (M) In Absorbance
- what weight of betazole phosphotungstate might be expected in the assay of 0.1550 g sample of betazole hydrochloride containing 98% C5H9N3.2HC? Gravimetric factor = 0.0909Q) water hardness of each trial and average ppm with calculation, please. Hard Water Trial 1 Hard Water Trial 2 Hard Water Trial 3 Initial Syringe Reading 1.0ml 1.0ml 1.0ml Final Syringe Reading 0.88ml 0.84ml 0.85ml Volume of EDTA Consumed 0.12ml 0.16ml 0.15ml Water Hardness ppm CaCO3 Average ppmFor Indirect Iodometric Analysis of Copper... ~0.0896g KIO3 necessary to consume 350mL of 0.1 M Na2S2O3, Na2S2O3 is stored in an amber glass bottle until ready for use. Primary Standard KIO3 has 2g of KI, 50mL of DI water, and 10 mL of 1.0M HCl is added then immediately titrated with Na2S2O3 until medium yellow or straw... then 5mL of starch indicator is added and titrated again until blue black color turns clear. Unknown CuO use 1.2G of Unknown, 20mL of HNO3 heated until sample dissolved, 25 mL of DI water added and boiled until clear light blue color, after cooling 1:1 NH3 added (~34.47 mL of NH4OH reagent) until permanent deep blue color amine complex, 2g of NH4HF2 added and swirled until dissolved, 3 g of KI is added then titrated immediately with Na2S2O3 until brown color of iodide is nearly gone (brown milk color), 2 g of KSCN and 3 mL of starch indicator is then added with titration continuing until disappearance of new blue black color. 1. Na2CO3 is often added to thiosulfate…