can you validate the synthesis of isoamyl acetate through the esterification reaction of isoamyl alcohol and acetic acid using the attached Carbon-13 NMR spectra. 13C NMR of isoamyl alcohol:200180160140120100ppm09-08060.9705060408-20-041.750024.83022.680 13C NMR of isoamyl acetate:171.080200180160440140120100ppm-8063.13060-60-40-37.48025.18022.510-20.960-0200

Please check below for the answer of the question. Explanation:The reaction must be: For the…

13C NMR of isoamyl alcohol: 200 180 160 140 120 100 ppm 09-0 80 60.970 50 60 40 8- 20 -0 41.750 0 24.830 22.680 13C NMR of isoamyl acetate: 171.080 200 180 160 440 140 120 100 ppm - 80 63.130 60 -60 - 40 -37.480 25.180 22.510 -20.960 -0 20 0

13C NMR of isoamyl alcohol: 200 180 160 140 120 100 ppm 09-0 80 60.970 50 60 40 8- 20 -0 41.750 0 24.830 22.680 13C NMR of isoamyl acetate: 171.080 200 180 160 440 140 120 100 ppm - 80 63.130 60 -60 - 40 -37.480 25.180 22.510 -20.960 -0 20 0

Introduction to General, Organic and Biochemistry

11th Edition

ISBN:9781285869759

Author:Frederick A. Bettelheim, William H. Brown, Mary K. Campbell, Shawn O. Farrell, Omar Torres

Publisher:Frederick A. Bettelheim, William H. Brown, Mary K. Campbell, Shawn O. Farrell, Omar Torres

Chapter16: Amines

Section: Chapter Questions

Problem 16.17P: 16-17 Propylamine (bp 48°C), ethylmethylamine (bp 37°C), and trimethylamine (bp 3°C) are...

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Question

can you validate the synthesis of isoamyl acetate through the esterification reaction of isoamyl alcohol and acetic acid using the attached Carbon-13 NMR spectra.

13C NMR of isoamyl alcohol:
200
180
160
140
120
100
ppm
09-0
80
60.970
50
60
40
8-
20
-0
41.750
0
24.830
22.680

13C NMR of isoamyl acetate:
171.080
200
180
160
440
140
120
100
ppm
-
80
63.130
60
-60
-
40
-37.480
25.180
22.510
-20.960
-0
20
0

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